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ACRYLONITRILE: METHOD 1604, Issue 2, dated 15 August 1994 - Page 4 of 4 REFERENCES: [1] Gagnon, Y.T. and Posner, J.C. Recovery of Acrylonitrile from Charcoal Tubes at Low Levels, Am. Ind. Hyg. Assoc. J., 40, 923-925 (1979). [2] NIOSH Manual of Analytical Methods, 2nd. ed., V. 3, S156, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-157-C (1977). [3] Criteria for a Recommended Standard...Occupational Exposure to Acrylonitrile, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 78-116 (1978); revised Mar, 1978 as part of NIOSH testimony at OSHA hearing. [4] NIOSH Manual of Analytical Methods, 2nd ed., V. 1, P&CAM 202, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-157-A (1977). [5] Marano, R.S., Levine, S.P. and T.M. Harvey. Trace Determination of Subnanogram Amounts of Acrylonitrile in Complex Matrices by Gas Chromatography with a Nitrogen Selective Detector. Anal. Chem., 50, 1948 (1978) [6] Documentation of the NIOSH Validation Tests, S156, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-185 (1977). [7] OSHA Report, Acrylonitrile Method 37, Organic Methods Evaluation Branch, OSHA Analytical Laboratory, Salt Lake City, UT (May, 1982).

METHOD REVISED BY: Y.T. Gagnon, NIOSH/DPSE; S156 originally validated under NIOSH Contract CDC-99-74-45.

NIOSH Manual of Analytical Methods (NMAM), Fourth Edition, 8/15/94