ORGANONITROGEN PESTICIDES: METHOD 5601, Issue 1, dated 15 January 1998 - Page 8 of 21 TABLE 2. METHOD EVALUATION Compound
Aldicarb Benomyl
LOD (µg/samp)
Mean Bias
Overall Precision ( rT)
Accuracy
12.0-240
1.2
-0.009
0.066
± 0.131
93.2
95.6
A
A
A
A
A
Storage Stability 31-Day %Rec. 24 C -12 C
12.0-120
0.6
Captan
30
48.0-960
4.8
-0.036
0.061
± 0.142
98.7
102.2
Carbaryl
6
12.0-240
0.06
+0.012
0.061
± 0.123
88.2
91.8
Carbendazim
6
0.6
+0.006
0.061
± 0.121
92.1
89.3
B
240
12.0-240
0.6
-0.020
0.060
± 0.126
89.1
92.4
Chlorpropham
6
12.0-240
0.6
-0.017
0.068
± 0.140
84.3
85.9
Diuron
3
12.0-240
0.6
-0.062
0.060
± 0.167
86.0
87.1
Formetanate.
60
12.0-240
0.6
+0.032
0.056
± 0.129
89.8
93.0
Methiocarb
60
12.0-240
0.6
+0.009
0.061
± 0.122
85.1
89.1
Methomyl
12
12.0-120
0.6
-0.002
0.063
± 0.124
90.5
95.2
240
12.0-240
0.6
+0.037
0.055
± 0.132
94.8
95.9
Propham
3
12.0-240
0.8
-0.053
0.066
± 0.168
88.5
92.5
Propoxur
60
12.0-240
0.6
+0.007
0.079
± 0.156
91.4
95.4
6
12.0-240
0.6
-0.068
0.073
± 0.197
75.0
79.8
Oxamyl
Thiobencarb
B
240
Range Studied (µg/samp)
6
Carbofuran
A
Min. Sample Vol (L)
Results calculated as carbendazim, the primary breakdown product of benomyl. See range for benomyl, a precursor for carbendazim.
NIOSH Manual of Analytical Methods, Fourth Edition
