Page:Experimental researches in chemistry and.djvu/263

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248
On the Manufacture of Optical Glass.'
[1829.

the glass is either transferred by a platinum ladle into trays roughly turned up out of old platina foil, or into a clean deep white earthenware vessel containing much distilled water. In the latter case it is obtained in a divided state, and when drained, is dried on the sand-bath, and put up in clean bottles.

29. When a crucible has been emptied of its first portion of glass, it will serve, if carefully used, for a second, third, fourth, or for many operations; but it should be watched for cracks and casualties, that the running of the glass into the furnace may be prevented, and, if necessary, another vessel taken.

30. The rough glass thus prepared is in the next operation to be converted into an annealed and finished plate. The size must therefore be determined upon, and we will assume it as 7 inches square, and 8 tenths of an inch thick, that being the dimension of the largest plate as yet made. For the purpose of making a competent platinum vessel, a plate of that metal will be required at least 10 inches square; but if larger, it should not be cut, but either made into a tray with higher sides than absolutely needful, or else used first in the manufacture of a larger plate of glass than the one to be described. It should be of such thickness as to weigh at least 17.5 grains to the square inch; and it is important that in its preparation a good ingot, or the good part of an ingot, of platinum has been selected, and that it has been rolled very gradually and care; fully without the formation of any holes by the adhesion of dirt or hard particles, or by the dragging of the metal in the mills. The desired perfection is, I understand, best obtained by rolling the platinum between two clean plates of good copper.

31. The plate, being laid upon clean paper or a cloth on a smooth table, is to be cleansed with a cloth and a little water or alcohol, and then to be ignited at every part by a large spirit-lamp. It must next be carefully examined as to its state, and the occurrence of places upon its surface where holes are likely to exist. If the metal seems dragged in any place, an effect indicated by a roughness upon the surface, or by short lines parallel to each other but perpendicular to the course of rolling, such place should be noted or marked, for which purpose a dot of ink will be convenient. If a scale appears, or a small portion is apparently folded over, it should also be marked; and if a black spot is visible (and they are sometimes